Uswatun Hasanah, Rusnadi, M. Bachri Amran

Judul	:	PRAKONSENTRASI DAN ANALISIS ION KADMIUM BERBASIS FLOW INJECTION ANALYSIS
Abstrak	:	CD-imprinted polymers (Cd-IPs) have been synthesized and retensinya properties have been studied for the pre concentration and analysis of cadmium concentration at the level of µ g L- 1berbasis technique of flow injection analysis (FIA). This procedure is based on the retention of ions Cd (II) on Cd-IPs are synthesized. Retention cadmium ions can elution quantitatively with a solution of nitric acid directly onto the nebulizer system for atomic absorption spectrometer. The retention capacity of the Cd-IPs acquired for 20.10 mg g-1pada pH optimum and shows a quick retention kinetics. Analytical parameters such as retention capacity, the volume of the sample, the concentration and volume of eluen have been evaluated to obtain a good analytical performance. The system being developed makes it possible to analyze 15 samples per hour, with a limit of detection of the 8 µ g L-1. For the concentration of 50 μg L-1 has obtained precision values expressed as percent relative standard deviation of 1.6 (n = 5). A method of analysis that was developed has been used for the determination of cadmium in river water samples Cidurian, West Java, Indonesia with satisfactory results. Key words: consentration, analyzing miniscule, cadmium, FIA
Tahun	:	2018	Media Publikasi	:	Jurnal Nasional Blm Akreditasi
Kategori	:	Jurnal	No/Vol/Tahun	:	2 / 15 / 2015
ISSN/ISBN	:	1411-9447
PTN/S	:	Pakuan	Program Studi	:	KIMIA
Bibliography	:	Almeida, J. A., Barreto, R. E., Novelli, L. B., Castro, F. J., and Moron, S. E.,“Oxidative Stress Biomarkers and Aggressive Behavior in Fish Exposed to Aquatic Cadmium Contamination”. Neotrop.Ichtyol., 2009, Vol 7, pp. 103-108.   47 Amran, M. B., Panggabean, A. S., Sulaeman, A. and Rusnadi, M,. “Preparation of a Chelating Resin and its Application as a Pre concentration System for Determination of Cadmium in River Water by Flow Injection Analysis”,Spring 2011, Int. J. Environ. Res., 5(2):531-536, ISSN: 1735-6865.   B. Welz, M. Sperling, “Atomic Absorption Spectrometry”, 3rd compl. rev. ed., Wiley-VCH, Weinheim, 1999. Flora, S. J. S.,“Metal Poisoning: Treatment and Management”. Review Article. Al Ameen, J. Med. Sci, 2009,Vol 2, pp. 4-26. Liu G., Freund M.S., New Approach for the Controlled Cross-Linking of Polyaniline: Synthesis and Characteization, 1997, Macromol., 30, p.5660. Panahi, Ahmad., Homayon., Samadi Zadeh., Marjaneh., Tavangari., and Simin. 2012. Nickel Adsorption from Enviromental Samples by Ion Imprinted Aniline-Formaldehyde Polymer. Islamic Azad University and Toosi University of Technology. Tehran : Iran. Vol. 31, No. 3. Patrick, L., “Toxic Metals and Anti- oxidants. Part II the Role of Anti-oxidant in Arsenic and Cadmium Toxicity – Toxic Metals part II”, 2003, Alternativer Medicine Review. PyrzyÅ„ska, K. and SzelÄ…g, H.,“On-line Preconcentration system with FAAS detection for determination of cadmium”, Anal.Lett., 2001, 34(12), 2153–2158 Rao, P.T., Daniel, S, Gladis, J.M.,“Tailored Materials for Preconcentration or Separation of Metals by Ion-Imprinted Polymers for Solid-Phase Extraction (IIPSPE)”,Trends in Anal. Chem., 2004, 23 (1): 29- 35. Sid Kalal, H, Hoveidi, H., Thagiof, M., Pakizevand, N., Almasian, M. R., and Firoozzare, M. A., “Pre-concentration and Determination of Platinum (IV) in Water Samples Using Chelating Resin by
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